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This book presents a detailed study on the design, synthesis, and characterization of novel achiral bent-core liquid crystals based on a four-ring benzene framework. It explores how structural modifications such as polar and non-polar substituents affect mesophase behavior, chirality and photophysical properties. Combining synthetic strategies with experimental techniques like DSC, POM, and X-ray diffraction, the book offers valuable insights into structure-property relationships in bent-core mesogens, making it a useful resource for researchers and students in materials science and liquid crystal research.